Nanoscale mechanisms of misfit dislocation propagation in undulated Si1-xGex/Si(100) epitaxial thin films

Chi-Chin Wu, University of Virginia
Eric A. Stach, School of Materials Engineering and Birck Nanotechnology Center, Purdue University
Robert Hull, University of Virginia

Date of this Version

April 2007

Citation

Nanotechnology 18 165705

This document has been peer-reviewed.

 

Comments

doi: 10.1088/0957-4484/18/16/165705

Abstract

Nanoscale lateral variations in the stress field of undulated Si0.7Ge0.3/Si(100) films have been experimentally studied via in situ transmission electron microscopy annealing and through finite element calculations. When annealed at ~480 °C, misfit dislocations in a 30 nm film (having surface undulations of ~70 nm wavelength and ~3 nm amplitude) propagated at 80 nm s−1 average speed but with periodic variations from 0–30 nm s−1 at the peaks of the undulations to 160–240 nm s−1 at the troughs. A 2.0 GPa average film stress with variations from 3.2 to 4.4 GPa at the troughs to 0.7–1.2 GPa at the peaks is inferred from the observed dislocation velocities. These stress variations are significantly higher than those calculated from a finite element model of Si0.7Ge0.3/Si with the same surface geometry. Using standard models of dislocation kink dynamics, we have calculated how the effect of high stresses at the undulation troughs would be expected to enhance kink nucleation rates, and have found good agreement between our models and the experimentally observed range of dislocation velocities. These observations demonstrate the potential of probing the nanoscale structure in thin films through local variations of dislocation velocities.

 

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